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Beilstein J. Org. Chem. 2022, 18, 746–753, doi:10.3762/bjoc.18.75
Graphical Abstract
Figure 1: Highly reactive dienophiles.
Figure 2: Dibromide substrates and product 12.
Scheme 1: Mechanochemical reaction of 10 with anthracene.
Figure 3: Scope of the Zn/Cu reaction with dibromide 10 (dienes are colored in red).
Scheme 2: Mechanochemical reaction of 11 with furan.
Scheme 3: Reactivity of bicyclo[2.2.2] dibromide 42 with dienes.
Beilstein J. Org. Chem. 2019, 15, 1313–1320, doi:10.3762/bjoc.15.130
Scheme 1: FCR of pyrene and phthalic anhydride.
Scheme 2: Scope of acylation reagents in FCR under mechanochemical activation conditions and comparison with ...
Scheme 3: Scope of aromatic substrates in FCR under mechanochemical activation conditions. aIsolated yields.
Scheme 4: Mechanochemical regiodirected FCR of anthracene dimer and succinic anhydride.
Scheme 5: Regioselectivity direction by protection of 9,10-anthracene ring positions.
Scheme 6: Double FCR of phthaloyl chloride and aromatics.
Figure 1: In situ Raman monitoring of reaction of phthalic anhydride with p-xylene.
Beilstein J. Org. Chem. 2017, 13, 1745–1752, doi:10.3762/bjoc.13.169
Scheme 1: N-Alkylation of imide 1 with 1,3-dibromopropane (2) in a ball mill.
Scheme 2: Mechanochemical N-alkylation of imide 1.
Figure 1: Products of alkylation of imides 11–17.
Figure 2: Ex situ IR spectroscopy of the reaction of 12 and benzyl bromide in the ball mill: a) phthalimide 12...
Scheme 3: Mechanosynthesis of 7,8-dimethylalloxazine (36) and its N-alkylation.
Scheme 4: Gabriel synthesis of amines in ball mill.
Scheme 5: Three-step, two-pot Gabriel synthesis of amines in ball mill.